Different Mathematical Spectrophotometric Methods for Determination of Ampyrone in Presence of Its Acid Degradation Product
DOI:
https://doi.org/10.23851/mjs.v31i3.778Keywords:
Area under curve, Ampyrone, simultaneous equation, modified simultaneous equation, Acidic product.Abstract
Three simple spectrophotometric methods namely; area under the curve, simultaneous equation method, and modified simultaneous equation method was developed and validated for the determination of Ampyrone with the presence of its acidic product using zero-order spectra without prior separation techniques. The linearity was found in the range of (10-50 mg/L) and (10-55 mg/L) for Ampyrone and its acidic product, respectively. The recovery percentage was found to be in the range from 99.6 to 100.65 for the area under curve method and 96.64 to 104.8 for the simultaneous equation method and its modified version which showed good accuracy and precision for three proposed methods.
Downloads
References
S.S. Saleh, S.M. Riad. 2018. Analytical Investigation on Green Smart Spectrophotometric Methods Utilizing Unified Regression Equation, 2008, Analytical Chemistry Letters, 8 : 268-76,
A. Parmar, S. Sharma. 2016. Derivative UV-vis absorption spectra as an invigorated spectrophotometric method for spectral resolution and quantitative analysis: Theoretical aspects and analytical applications: A review, TrAC Trends in Analytical Chemistry. 77: 44-53.
M. M. Abdelrahman. 2013. Simultaneous determination of Cinnarizine and Domperidone by area under curve and dual wavelength spectrophotometric methods Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy. 113: 291-296.
I. H. Ibraheem, W.A. Mahmoud. 2014. Synthesis and Spectral Analysis of Mn (II), Cu (II), Ni (II) and Cd (II) Complexes with Mixed Ligands containing 1, 10-phenanthroline and Schiff base derived of 4-aminoantipyrine. Baghdad Science Journal. 1:1519-1527.
R. K. Al-Shemary, A. L. Niseaf, A. J. Jarad. 2017. Synthesis, characterization and antibacterial Evaluation for mixed-ligand Complexes of Nickle (II), Manganese(II), Copper(II),Cobalt(II) and Mercury(II) with Tetradentate Schiff base and 1,10-phenanthroline . Al-Mustansiriyah Journal of Science. 28(2): 80-85.
J.J. Xiong, P.C. Huang, C.Y. Zhang, F.Y. Wu. 2016. Colorimetric detection of Cu2+ in aqueous solution and on the test kit by 4-aminoantipyrine derivatives. Sensors and Actuators B: Chemical. 226: 30-6.
S. Manjula, S. Khan, A.A. Syed, S. Thanoi, C. Tocharus, S. Nudmamud-Thanoi, P. Sobhon, A.Samontha, W. Waiyawat, J. Shiowatana, R.G. McLaren. 2007. 4-Aminoantipyrine as a new electrophilic coupling reagent for spectrophotometric determination of iron (III) in water, industrial effluent and soil samples. Sci Asia. 33: 455-60.
J.M. Hong, J.K. Jun, H.Y. Kim, S. Ahn, S.K . Chang. 2015. Colorimetric signaling of Cu (II) ions by oxidative coupling of anilines with 4-aminoantipyrine. Tetrahedron letters, 56(40): 5393-5396.
H.Y. Kim, H.J. Lee, S.K. Chang. 2015. Reaction-based colorimetric signaling of Cu2+ ions by oxidative coupling of phenols with 4-aminoantipyrine. Talanta, 132: 625-629
I. Nukatsuka, S.Nakamura, K. Watanabe, K. OHZEKI. 2000. Determination of phenol in tap water and river water samples by solid-phase spectrophotometry. Analytical sciences, 16(3): 269-273.
J. I. Gowda, A. T. Buddanavar, S. T. Nandibewoor2015. Fabrication of multiwalled carbon nanotube-surfactant modified sensor for the direct determination of toxic drug 4-aminoantipyrine. Journal of pharmaceutical analysis, 5(4): 231-238.
J. I. Gowda, T. Sharanappa, Nandibewoor. 2012. Electrochemical behavior of 4-aminophenazone drug at a graphite pencil electrode and its application in real samples. Industrial & Engineering Chemistry Research, 51(49): 15936-15941.
E. Dabek-Zlotorzynska.1997. Capillary electrophoresis in the determination of pollutants. Electrophoresis, 18(12-13): 2453-2464.
D. Puig, I. Silgoner, M. Grasserbauer, D. Barcelo. 1997. Part-per-trillion level determination of priority methyl-, nitro-, and chlorophenols in river water samples by automated on-line liquid/solid extraction followed by Liquid chromatography/mass spectrometry using atmospheric pressure chemical ionization and ion spray interfaces. Analytical Chemistry, 69(14): 2756-2761.
R. F. Abbas. 2018. Two Derivative Spectrophotometric Methods for the Simultaneous Determination of 4-AminoAntipyrine in Presence of Its Acidic Products. Ibn AL-Haitham Journal For Pure and Applied Science, 31(2): 86-96.
K. A. Attia, N. M. Elabasawy, E. Abolmagd. 2017. Simultaneous equation and area under the curve spectrophotometric methods for estimation of cefaclor in presence of its acid induced degradation product; A comparative study. Future Journal of Pharmaceutical Sciences, 3(2): 163-167
M. A. Hegazy, A. M. Yehia, A.A. Mostafa. 2012. Stability-indicating methods for the determination of mosapride citrate in the presence of its degradation products according to ICH guidelines. Drug testing and analysis, 4(2): 104-115.
19. H.M. Lotfy, Y.M. Fayez, S.M Tawakkol., N.M.Fahmy, M.A. Shehata2017. Spectrophotometric determination for the binary mixture of clotrimazole and dexamethasone in pharmaceutical dosage form. Analytical Chemistry Letters, 7(1): 30-42.
R.F. Abbas, H.A. Abbas, M.M. Rawa, D.A. Abdulabbas, M.A. Abed. 2017. Estimation of the Folic Acid Using Zero Order, Area Under Curve and First Derivative Spectrophotometric Methods in Pure and Marketed Tablet Formulations. Al-Nahrain Journal of Science, 20(3): 34-41.
B.M. Ayoub. 2016. Development and validation of simple spectrophotometric and chemometric methods for simultaneous determination of empagliflozin and metformin: Applied to recently approved pharmaceutical formulation. Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy, 168: 118-122.
L. Kalyani, C. V. Rao, 2018. Simultaneous spectrophotometric estimation of Salbutamol, Theophylline and Ambroxol three component tablet formulation using simultaneous equation methods. Karbala International Journal of Modern Science, 4(1): 171-179.
N. Erk, F. Onur. 1997. Three new spectrophotometric methods for simultaneous determination of hydrochlorothiazide and amiloride hydrochloride in sugar-coated tablets. Analytical letters, 30(8): 1503-1515.
A. M. Al Alamein, H.M. Elwy, S.H.El-Din, 2019. Univariate and multivariate spectrophotometric methods for simultaneous determination of avobenzone and octinoxate in pure form and in cosmetic formulations: A comparative study. Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy, 206: 37-47.
Downloads
Key Dates
Published
Issue
Section
License
Articles accepted for publication in Al-Mustansiriyah Journal of Science (MJS) are protected under the Creative Commons Attribution 4.0 International License (CC BY-NC). Authors of accepted articles are requested to sign a copyright release form prior to their article being published. All authors must agree to the submission, sign copyright release forms, and agree to be included in any correspondence between MJS and the authors before submitting a work to MJS. For personal or educational use, permission is given without charge to print or create digital copies of all or portions of a MJS article. However, copies must not be produced or distributed for monetary gain. It is necessary to respect the copyright of any parts of this work that are not owned by MJS.
How to Cite
